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The proton‐bound dicarboxylate motif, RCOO−⋅H+⋅−OOCR, is a prevalent chemical configuration found in many condensed‐phase systems. The proton‐bound formate dimer HCOO−⋅H+⋅−OOCH was studied utilizing cold‐ion IR action spectroscopy in the range 400–1800 cm−1. The spectrum obtained at ca. 0.4 K of ions captured in He nanodroplets was compared to that measured at ca. 10 K by photodissociation of Ar‐ion...
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