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We report on the asymmetric occupation of a 12‐vertex cluster centered by a single metal atom. Three salts of related intermetalloid cluster anions, [Co@Sn6Sb6]3− (1), [Co2@Sn5Sb7]3− (2), and [Ni2@Sn7Sb5]3− (3) were synthesized, which have pseudo‐C4v‐symmetric or pseudo‐D4h‐symmetric 12‐vertex Sn/Sb shells and interstitial Co− ions or Ni atoms. Anion 1 is a very unusual single‐metal‐“centered” 12‐atom...
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