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The coordination polymers [M(dca) 2 pyz] (M=Mn, Fe, Co, Ni, Zn) have been synthesized and characterized by single-crystal and powder X-ray diffraction. Two isomers have been observed. The α compounds contain two interpenetrating 3D α-Po related networks. Bidentate dca ligands bridge the metal atoms to form square-grid-like M(dca) 2 sheets, with the pyrazine ligands linking these sheets...
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