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Nine partially halogenated benzylphosphanes ArXCH2PR2 (ArX = 3,6‐dichlorophenyl, 3,6‐difluorophenyl and 3,4,5‐trifluorophenyl; R = Ph, Cy, iPr) have been prepared and reacted with palladium acetate to obtain the cyclometallated dimers [Pd(µ‐OAc)(κ2‐C,P‐ArXCH2PR2)]2. The acetate bridge has been exchanged by bromide using lithium bromide and the obtained dimers have been thoroughly characterised. The...
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