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The electrochemical behavior of the stepped electrodes vicinal to the Pt(100) surface in bromide containing solutions has been studied by cyclic voltammetry, STM and the CO displacement method. The studied electrodes belong to the [011] and [001] zones, which nominally have n atom-wide terraces with (100) symmetry and (111) or (100) monoatomic steps, respectively. The voltammetric behavior of these...
The effect of three surface electrochemical preparation techniques for single crystal surfaces on two platinum stepped surfaces [Pt(10,10,9) and Pt(11,10,10)] has been investigated by scanning tunneling microscopy and cyclic voltammetry. The preparation techniques consisted of a thermal treatment followed by a cooling step in (a) a hydrogen+argon atmosphere, (b) air (c) iodine vapor+air. For Pt(10,10,9)...
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