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Reductive aromatization of perylene diimides with acid anhydrides in the presence of Mn or Zn metals provides soluble and planar 2,9‐diazaperopyrenes with ester groups at 1,3,8,10‐positions. The pivaloxy groups at the peripheral positions can be transformed into a variety of aryl groups through nickel‐catalyzed cross‐coupling of ester groups. Emission colors of diazaperopyrenes are tunable by the...
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