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Unsolvated potassium 9-triphenylsilylfluorenide, [KFl(SiPh 3 )] n (3, Fl = fluorenyl), has been prepared in 89% yield by metalation of 9-fluorenyltriphenylsilane (2) with potassium hydride in toluene/THF and structurally characterized by X-ray diffraction. In the solid state, compound 3 comprises a linear chain structure. Due to the absence of coordinating solvent molecules, supramolecular...
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