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A new heteronuclear NMR pulse sequence for the measurement of nJ(C,H) coupling constants, the α/βselective HC(C)H-TOCSY, is described. It is shown that the S3E element (Meissner et al., 1997a,b) can be used to obtain spin state selective coherence transfer in molecules, in which adjacent CH moieties are labeled with 13C. Application of the α/β selective HC(C)H-TOCSY to a 10nt RNA tetraloop 5′-CGCUUUU...
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