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The use of Pd catalysis as a means to synthesize organic halides has recently received increased attention. Among the reported methods is the Pd‐catalyzed carboiodination, which uses extremely bulky ligands to facilitate carbon–halogen reductive elimination from PdII as the key catalytic step. When approaching substrates exhibiting low stereoselectivity, catalyst troubleshooting becomes difficult...
So oder so: Bedingungen für die intramolekulare Carboiodierung und für die simultane konvergente intramolekulare Carboiodierung/intermolekulare Heck‐Reaktion von Diiodarenen wurden entwickelt. Dank der Fähigkeit der Katalysator/Ligand‐Kombination Pd0/QPhos, eine reversible oxidative Addition einzugehen, laufen diese Reaktionen gut ab, was den Nutzen dieser Substratklasse bei regioselektiven Kreuzkupplungen...
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