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Adsorptive separation of acetylene from ethylene/acetylene mixtures is a technologically very important and highly challenging task. In this work, we describe two flexible metal–organic frameworks (MOFs), ELM‐11 and ELM‐13, that display adsorbate discriminatory gate effects. The two MOFs exhibit gate‐opening‐type adsorption properties for C2H2 but not for C2H4, leading to a highly selective adsorption...
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