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Acetylene, an important petrochemical feedstock, is the starting chemical to produce many polymer products. Separating C2H2 from its by‐product mixtures is still an energy‐consuming process and remains challenging. Here, we present a metal–organic framework[Zn2(bpy)(btec)], with a desirable pore geometry and stable framework, which demonstrated a high separation performance of C2H2 from simulated...
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