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Interconversion of the molybdenum amido [(PhTpy)(PPh2Me)2Mo(NHtBuAr)][BArF24] (PhTpy=4′‐Ph‐2,2′,6′,2“‐terpyridine; tBuAr=4‐tert‐butyl‐C6H4; ArF24=(C6H3‐3,5‐(CF3)2)4) and imido [(PhTpy)(PPh2Me)2Mo(NtBuAr)][BArF24] complexes has been accomplished by proton‐coupled electron transfer. The 2,4,6‐tri‐tert‐butylphenoxyl radical was used as an oxidant and the non‐classical ammine complex [(PhTpy)(PPh2Me)2...
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