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In this work, we report that 2‐cyano‐2‐phenylpropanoic acid and its p‐Cl, p‐CH3 and p‐OCH3 derivatives can be used as chemical fuels to control the geometry of the calix[4]arene scaffold in its cone conformation. It is shown that, under the action of the fuel, the cone calix[4]arene platform assumes a “locked” shape with two opposite aromatic rings strongly convergent and the other two strongly divergent...
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