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Cobalt‐assisted hydrosilylation of acetylenes is particularly interesting in organic synthesis since alkynyl group functionalization can give way to more useful substructures. This study aims to answer the general question of how to control hydrosilylation regioselectivity with unsymmetric alkynyl groups. Cobalt‐catalyzed hydrosilylation is highly regioselective with alkyl‐phenylthio‐acetylenes affording...
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