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Procedures are described for the synthesis of complexes containing the cations [Cu 2 (μ-OR)(μ-O 2 CMe) 2 (bpy) 2 ] + (R = Me, Et, Pr n ). Treatment of Cu 2 (O 2 CMe) 4 (H 2 O) 2 with 2 equivs of bpy and 1 equiv. of NaOH in anhydrous EtOH, followed by addition of NBu n4 PF 6 in MeCN gave highly...
The monoindenyl species [(η 5 -C 9 H 7 )ZrCl 3 ] n and [(η 5 -C 9 H 7 )HfCl 2 (μ-Cl)] 2 have been prepared. The structurally characterized hafnium dimer represents the first structurally characterized Cp (or substituted Cp) hafnium trichloride complex.
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