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Metal–organic polyhedra (MOPs) or frameworks (MOFs) based on Cr3+ are notoriously difficult to synthesize, especially as crystals large enough to be suitable for characterization of the structure or properties. It is now shown that the co‐existence of In3+ and Cr3+ induces a rapid crystal growth of large single crystals of heterometallic In‐Cr‐MOPs with the [M8L12] (M=In/Cr, L=dinegative 4,5‐imidazole‐dicarboxylate)...
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