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The preparation of organometallic oxides, imides and nitrides is described. The molecular structures of these compounds resemble those found in binary systems. However, due to the organic envelope of the molecular solids, they are soluble in organic solvents, easy to crystallize and unambiguously characterizable by single X-ray structural analysis and NMR investigations. Moreover, inorganic oxides...
Trivalent iron complexes which could be easily converted into materials are formed by the reaction of FeCl 3 with K 3 [O 3 SiMe] in a highly concentrated aqueous alkaline solution. The presence of the liquid glass as an additive and decreasing the pH results in solutions that give rise to homogeneous gels. Polycondensation proceeds very rapidly in the higher pH range (viz....
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