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Diphenyldiazomethane reacts with HB(C6F5)2 and B(C6F5)3, resulting in 1,1‐hydroboration and adduct formation, respectively. The hydroboration proceeds via a concerted reaction involving initial formation of the Lewis adduct Ph2CN2BH(C6F5)2. The highly sensitive adduct Ph2CN2(B(C6F5)3) liberates N2 and generates Ph2CB(C6F5)3. DFT computations reveal that formation of Ph2CN2B(C6F5)3 from carbene, N2...
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