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Iron(II) complexes of 1,2-bis(diallylphosphino)ethane (TAPE) were explored as a possible route to polymeric materials that would reversibly bind N 2 and H 2 . A new synthetic route to the TAPE ligand was developed. Starting with the trans-Fe(TAPE) 2 Cl 2 complex, a series of iron(II) complexes was synthesized having the general formula FeL 2 (A)(B) where L=TAPE...
The biomedically useful Cu(DHMPE) 2+ complex (DHMPE=1,2-bis[(dihydroxymethyl)phosphino]ethane, a water-soluble bidentate phosphine) is normally synthesized from expensive Cu(I) sources because the use of cheaper CuCl can lead to a variety of unwanted coordination complex by-products. A method is reported for the synthesis of Cu(DHMPE) 2+ from CuCl. Reaction of CuCl with DHMPE...
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