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The synthesis of [AgO2CCR2OC(O)OMe] (6, R = H; 7, R = Me) by treatment of HO2CCR2OC(O)OMe (4, R = H; 5, R = Me) with [AgNO3] in presence of NEt3 is reported. The reaction of 6 and 7 with 2 equiv of PPh3 gave [AgO2CCR2OC(O)OMe(PPh3)2] (8, R = H; 9, R = Me). The thermal behavior of 6 and 7 was studied by TG, DSC and TG-MS of which the latter evinced decarboxylation as initial decomposition step followed...
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