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MesP(H)SiCl2Ph (Mes = 2,4,6‐Me3C6H2) (7) with a reactive Si–Cl and P–H bond can easily be reduced by KC8 or alternatively by a carbene to give remarkable phosphorus silicon compounds. 7 is readily synthesized from the reaction of MesPH2 sequentially with nBuLi and PhSiCl3 in a 1:1:1 ratio. KC8 reduction of MesP(H)SiCl2Ph (7) in the presence of cyclic alkyl(amino) carbene (cAACMe) gives (MesPH)3SiPh...
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