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The control of radical reactions to afford selective carbon–carbon bond formation is a significant synthetic challenge with applications ranging from small‐molecule activation to natural product synthesis. Oxidation of (IP–)2Al(CH3) (1, IP = iminopyridine) with TrBPh4 (Tr = trityl) afforded the C–C coupled product [(IP)(Tr‐IP)Al(CH3)][BPh4] (2) in which the trityl radical and the IP– radical have...
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