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Addition of two equivalents of tris(2-hydroxy-3,5-dimethylbenzyl)amine (H3Lig) to the solution of MoO2(acac)2 in MeOH results in the formation of anionic complex, which precipitates as LigH4[MoO2Lig], a yellow crystalline solid. Crystal structure determinations reveal that the asymmetric unit consists of one [MoO2Lig]− anion, one H4Lig+ cation and two molecules of solvent. Three phenoxide groups of...
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