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The reaction of ReH 92- with Mo(diglyme)(CO) 3 leads to the formation of the mixed metal cluster trianion, ReMo 3 H 4 (CO) 123- . This species has been characterized analytically, spectroscopically and through X-ray diffraction analysis. A pseudo-tetrahedral arrangement of M(CO) 3 fragments is adopted, such that each set of...
The reactions of [(H 5 C 6 ) 3 P] 2 ReH 6- with (CH 3 CN) 3 Cr(CO) 3 , (diglyme)Mo(CO) 3 or (C 3 H 7 CN) 3 W(CO) 3 led to the formation of [(H 5 C 6 ) 3 P] 2 ReH 6 M(CO) 3- (M = Cr, Mo, W) complexes. These have been characterized by IR and...
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