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We present a modeling scheme to analyze cagelike silica mesoporous crystals based on in situ X‐ray diffraction (XRD) data collected during gas adsorption–desorption (physisorption) processes. Nitrogen physisorption on a silica mesoporous crystal of SBA‐16 was directly monitored by using synchrotron in situ powder XRD measurements conducted at SPring‐8. SBA‐16 is a well‐ordered mesoporous silica in...
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