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The highly stereoselective synthesis of d,l-hexestrol (1), an inhibitor of microtubule assembly, is developed by using, as a key step, an intermolecular coupling of Co 2 (CO) 6 -complexed propargyl radicals. The latter are generated by novel complementary processes involving an interaction of tetrahydrofuran with Co 2 (CO) 6 -complexed propargyl alcohols and cations...
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