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NMR‐Spektroskopie großer Proteinsysteme gelingt nur nach gezielter Protonierung ausgewählter Positionen vor einem perdeuterierten Hintergrund. In der Zuschrift auf S. 2002 ff. von J. Boisbouvier et al. wird eine Acetolactatvorstufe vorgestellt, um biosynthetisch 13C1H3‐Gruppen spezifisch in die pro‐S‐Methyl‐Positionen von Leucin und Valin einzuführen. Dieses Markierungsverfahren verbessert die Spektrenqualität...
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