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Two new members of the hexanuclear series [Co6S8(PR3)6]n+, complexes [Co6S8(PMe2Ph)6](ClO4) (1) and [Co6S8P(OMe)36] (2), have been synthesizes and characterized by X-ray diffraction analyses. Their formation process was postulated to go through trinuclear μ3--S bridged moieties. The structural characteristics of the M6E8P6 skeleton of a whole series of [M6E8(PR3)6]n+ (M=Co, Cr, Fe, Mo; E=S, Se,...
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