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The oxidation of NADH is readily obtained in the presence of Dawson-type heteropolyanions (HPA). A stoichiometry of 2:1 is established for the oxometalate/NADH couple. The starting system for electrochemistry studies consists of the one-electron reduction product of the heteropolyanions in the presence of various amounts of NADH. The quantitative study by cyclic voltammetry confirms that the oxidized...
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