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Two novel alkali/alkaline‐earth borates, Ba6[B6O9(OH)6]2(H3BO3) (1) and Li7MAlB12O24 (M=Ba, Sr, Ca) (2 a–c), with 1D and 3D structures have been made hydrothermally and characterized. 1 features a rare 1D anionic chain built by hexaborate clusters of B6O11(OH)6; each made of six BO4/BO2(OH)2 tetrahedra. The anionic chains are embedded in the channels of a Ba6‐based wheel‐cluster open‐framework. On...
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