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The complex [PtMe 2 (TPMA)] (1), TPMA=tris(2-pyridylmethyl)amine, contains bidentate TPMA with two free pyridyl groups. It reacts with HX (X=CF 3 CO 2 , CF 3 SO 3 , BF 4 ) at room temperature to yield [PtHMe 2 (TPMA)][X], which exists as an equilibrium mixture of two isomeric forms, each containing fac-tridentate TPMA. The major product has the...
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