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A poly(N-methylaniline) (PNMA) film was obtained by chronoamperometry on tin oxide (TO) in dimethylformamide DMF containing 0.5M sulphuric acid. The PNMA film formation was monitored by in situ UV–vis spectroscopy. A detailed electropolymerization mechanism and reaction pathway of N-methylaniline (NMA) is proposed based on mass spectroscopy (MS) and NMR analysis. The NMA repeating units (both in the...
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