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Uniform pure iron (Fe) nanocrystals with particle size smaller than 10nm were synthesized via hydrogenation reduction of a nontoxic organometallic precursor ferric acetylacetone [Fe(acac)3] in an autoclave at elevated temperature. Since reaction is conducted with a pressure of 6MPa, choice of solvent become more convenient because some low-boiling-point solvents could also be used. In order to better...
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