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In order to study the crystal structure of β‐Ca2SiO4, time-of-flight neutron powder diffraction experiments were carried out at temperatures between room temperature (RT) and 600°C. Rietveld refinement at RT has shown that β‐Ca2SiO4 is monoclinic based on P2 1 /n symmetry and two different types of Ca sites, Ca(1) and Ca(2). All interatomic distances within 3Å were calculated, with the valences...
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