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A powder sample of a metastable phase β-MoSi 2 having the C40-type crystal structure was prepared by heating Mo sheets with a Na–Si melt at 858 K for 12 h to determine details of the crystal structure. The lattice constants (a = 4.6016(3) Å and c = 6.5700(3) Å) and Si atom coordinate (y = 0.1658(2)) of β-MoSi 2 were determined by Rietveld analysis of the X-ray powder diffraction. The...
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