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Rose-like crystalline particles of ammonium vanadium sulfate hydroxide (NH 4 V 3 (OH) 6 (SO 4 ) 2 ) were synthesized by a solvothermal route using dimethyl sulfoxide (DMSO)–water as the solvent. Following a thermal decomposition process, rose-like V 2 O 5 micro-architectures were fabricated via the in situ generated single-crystalline nanoparticles...
Hollow V 2 O 5 microspheres consisting of closely packed particles, radially aligned rods and randomly packed platelets were fabricated via calcining the as-synthesized precursors prepared by a solvo-thermal route using NH 4 VO 3 and oxalic acid as reagent and THF as solvent. SEM, TEM, XRD, XPS and UV–vis diffuse reflectance were used to characterize the fabricated...
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