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For the synthesis of a new functional polyisocyanate, the anionic polymerization of 3‐chloropropyl isocyanate (3CPIC) was carried out using several initiator systems in THF at −98 °C. When a sodium benzanilide (Na‐BA) cluster was used as an aggregated initiator, the initiation efficiency and polymer yield were low due to too fast propagation and cyclic trimerization compared to the initiation. A more...
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