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The synthesis and structural characterization of new tantalum(V) compounds containing a single hydrazido(I) ligand are reported. Hydrazinolysis of TaCl(NMe 2 ) 4 using trimethylsilyl(dimethyl)hydrazine affords the compound TaCl(NMe 2 ) 3 [N(TMS)NMe 2 ] in essentially quantitative yield. Metathetical replacement of the chloride ligand in TaCl(NMe 2 )...
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