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We report a new synthesis route towards polycrystalline Ba2FePnSe5 (Pn = Sb, Bi) chalcogenides based on ball milling and subsequent spark plasma sintering. The polycrystalline samples were characterized by transmission electron microscopy and powder X-ray diffraction. We discovered that both compounds undergo rapid, radiation induced phase changes between a crystalline and an amorphous phase. Thin...
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