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Amphiphilic diblock copolymer with an azobenzene linkage has been synthesized by the combination of macromolecular azo coupling reaction and nitroxide-mediated radical polymerization (NMP). In this strategy, an azobenzene linkage would naturally establish at the copolymer junction of the amphiphilic diblock copolymer after the macromolecular azo coupling reaction. Self-assembly of this azobenzene...
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