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In order to gain a better understanding of the parameters affecting the capacity and performance of spinel electrode materials, the chemical composition and cation distribution of three members of the LiCuxMn2xO4 and LiCu0.5yAlyMn1.5O4 series have been studied by chemical analysis, X-ray diffraction and X-ray absorption spectroscopy. The synthesis used stoichiometric and lithium-excess precursors...
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