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The new compound HP‐KB3O5 was synthesized under high‐pressure/high‐temperature conditions. It is the first compound exhibiting all three possible conjunctions simultaneously: corner‐sharing BO3 groups, corner‐sharing BO4 units, as well as edge‐sharing BO4 tetrahedra. Calculations of harmonic vibrational frequencies and 11B solid‐state NMR measurements were performed for the first time with a compound...
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