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Electrochemical oxidation of Bi-substituted phase La 2−x Bi x CuO 4 (x=0, 0.03 and 0.08) has been performed by using alkali metal hydroxide as an electrolyte. From X-ray Diffraction analysis, a structural transformation from orthorhombic to more distorted orthorhombic and to tetragonal could be observed for x =0 and 0.03, respectively, with c-axis elongation and unit cell expansion...
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