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We present a new co-casting method to synthesize novel mesostructured NiO/C composites with NiO nanoparticles studded in the wall of ordered mesoporous carbon materials. Ni 2+ ions were captured by the framework of partially polymerized sucrose in the channel of mesoporous silica; during the carbonization process, Ni(NO) 2 ·6H 2 O was decomposed and NiO nanoparticles was formed...
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