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Amongst the derivatives of 4‐biphenylcarboxylic acid and amino acid esters, the crystal structure of 4‐biphenylcarboxy‐(l)‐phenylalaninate is unusual owing to its monoclinic symmetry within a pseudo‐orthorhombic crystal system. The distortion is described by a disparate rotational property around the chiral centers (ϕchiral ≃ −129° and 58°) of the two molecules in the asymmetric unit. Each of these...
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