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The binding of three nucleobase-modified β-CDs, (i.e., mono(6-ade-6-deoxy)-β-CD 2, mono(6-thy-6-deoxy)-β-CD 3, and mono(6-ura-6-deoxy)-β-CD 4) with four bile salts (deoxycholate, DCA; cholate, CA; glycocholate, GCA; and taurocholate, TCA) were investigated by means of circular dichroism, 2D NMR spectroscopy and calorimetric titration. The results show the binding of host 2 with bile salts is weaker...
Calorimetric titration and NMR experiments in aqueous phosphate buffer (pH 7.2) at 298.15K have been done to determine the binding mode, complex stability constants and thermodynamics (ΔG°, ΔH°, and TΔS°) for 1:1 inclusion complexation of water-soluble calix[n]arenesulfonates (CnAS, n=4 and 6) and thiacalix[4]arene tetrasulfonate (TCAS) with acethylcholine, carnitine, betaine and benzyltrimethylammonium...
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