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Metastable hexagonal molybdenum trioxide has been synthesized by chemical precipitation and hydrothermal treatment at low temperature. X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and scanning electron microscopy (SEM) were used to characterize the product, which has a unique hexagonal prism-like morphology. Excellent electrochemical performances were exhibited: the first reversible...
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