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Chirality patterns are commonly observed in the universe and in nature, particularly at micro‐ and macrolevels governing the origin of life on earth. Multilayer folding 3D chirality was discovered as a new addition to the chirality family, which is now achieved at a macromolecular level through asymmetric catalytic polymerization. These polymers show conformational flexibility upon pushing and releasing...
Unprecedented chiral multilayer folding 3D polymers have been assembled and regulated by uniform and differentiated aromatic chromophore units between naphthyl piers. Screening catalysts, catalytic systems and monomers were proven to be crucial for asymmetric catalytic Suzuki–Miyaura polycouplings for this assembly. X‐ray crystallography of the corresponding dimers and trimers revealed the absolute...
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