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Solid structures of the compositionally fractionated bacterial poly(3-hydroxybutyric acid-co-3-hydroxypropionic acid)s [P(3HB-co-3HP)], bearing much narrower comonomer compositional distributions, were studied by high-resolution solid-state 13 C n.m.r. 1 H– 13 C cross-polarization relaxation behaviour (T CH and T 1ρH ) of chain-carbon nuclei was found to...
Two different kinds of natural poly(3-hydroxybutyric acid-co-3-hydroxypropionic acid)s [P(3HB-co-3HP)] with individual 3HP comonomer contents of 36.5 and 68.1 mol.% were biosynthesized by the bacteria Alcaligenes latus, fed on the cosubstrates of (R)-3-hydroxybutyric acid (3HBA) and 3-hydroxypropionic acid (3HPA). Employing the mixed chloroform/n-heptane solvent, the bacterial products were found...
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