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The reaction of 2‐(4‐methyphenyl)ethyl tosylate (Me-1-OTs) in 50/50 (v/v) trifluoroethanol/water at 25 °C is first order in the concentration of azide anion nucleophile. A carbon‐13 NMR analysis of the products of the reactions of Me‐1‐[α‐13C]OTs in 50/50 (v/v) trifluoroethanol/water at 25 °C shows the formation of Me‐1‐[β‐13C]OH, Me‐1‐[β‐13C]OCH2CF3 and Me-1-[β-13C]N3 from the trapping of a symmetrical...
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